OpenArsenic Quick Start Guide

Table of Contents

Part 1: Welcome to OpenArsenic
A brief introduction to the guide and expected users.
Part 2: Safety First
Gneral safety guidance including PPE, handling acids and arsenic-containing waste.
Part 3: What you need before you begin
This Materials section contains lists of required and optional equipment and consummables.
Part 4. Understanding the full workflow
Arsenic measurements follow the same basic workflow from preparing reagents to reviewing data.
Part 5: Setting up your workspace
Goal: Prepare a clean and organized workspace to do arsenic analysis.
Part 6: Setting up the Rodeostat and electrodes
How to assemble and connect hardware required for arsenic measurement using the Rodeostat potentiostat system.
Part 7: Installing & Opening OpenVoltam
OpenVoltam is the software used for potentiostat control, data collection, peak analysis, and arsenic concentration calculation.
Part 8: Preparing Solutions
This section describes the routine solutions needed for total arsenic measurements.
Part 9. Conditioning the gold electrode
Objective: clean and re-activate the working electrode surface to ensure stable arsenic measurements.
Part 10. Preparing a groundwater sample
Sampling may seem simple, but it is one of the most critical steps in ensuring that analytical results are meaningful.
Part 11. Running your first arsenic measurement
Objective: quantify dissolved arsenic via stripping voltammetry and standard addition.
Part 12. Analyzing peaks in OpenVoltam
OpenVoltam automatically estimates peak location, baseline, and endpoints, with the user verifying the analysis.
Part 13. Calculating arsenic concentration by standard addition
Complete the sample run, the first standard addition, and the second standard addition.
Part 14. Steps at the end of measurements
Proper cleaning and storage of the OpenArsenic system helps maintain measurement performance.
Part 15. Quality control and acceptance criteria
Data analysis criteria for conditioning, measurements and standard addition steps.
Part 16. Troubleshooting
This troubleshooting section includes recommended actions.
Part 17. Best practices for routine use
List of best practices and recommended daily routine.
Part 18. Glossary
Term Meaning OpenArsenic Complete open-source arsenic measurement platform. OpenVoltam Software used for data acquisition, peak analysis, and concentration calculation. Rodeostat Low-cost open hardware potentiostat used to run electrochemical measurements. Working electrode Electrode where arsenic is deposited and measured; gold microwire in this method. Reference electrode Electrode that provides